ID (ISN) del documento | 51404 |
Número CIS |
89-576 |
ISSN - Título de la serie |
0016-9900 - Gigiena i sanitarija |
Año |
1987 |
Número de serie |
|
Autor(es) |
Moraru L.E., Girenko D.B., Klisenko M.A. |
Título |
Chromatographic methods of determination of nitrogen and phosphorus-containing pesticides in air |
Título original |
Hromatografičeskie metody opredelenija azot-fosforsoderžaščih pesticidov v vozduhe [en ruso] |
Información bibliográfica |
Apr. 1987, No.4, p.53-54. Illus. 4 ref. |
Resumen |
Conditions were determined for the collection, separation and quantitation of 4 organophosphorus pesticides that may be present in workplace air. 20L of air is drawn through a paper disc backed by polyurethane foam. The disc and foam are extracted with acetone and the extract is concentrated. A sample of the concentrate may be subjected to gas chromatography on a column of 5% Se-30 on Chromaton N-AW at 190 or 210°C (flame photometric or thermal ionisation detector), or to thin-layer chromatography on silica gel with hexane-acetone mixtures; after visualisation of spots with Dragendorff's reagent or silver nitrate, the diameters of the spots are measured. The limit detection in air of actellic, pirimiphos ethyl and pyridafenthion is 0.1mg/m3; for hostaquick, 0.2mg/m3. Error limits are 15.5-19.6%. |
Descriptores (primarios) |
hostaquick; pesticidas; toma de muestras y análisis; dosificación en el aire; pirimifós etilo; cromatografía por gas líquido; cromatografía en capa delgada; pirimifós-metil; piridafentión |
Descriptores (secundarios) |
valoración de la higiene del trabajo; valoración del método |
Tipo de documento |
D - Artículos periódicos |
Tema(s) |
Agricultura, pesca, cría de ganado
|
Broad subject area(s) |
Riesgos químicos
|
Navegación por categoria(s) |
Esters and salts Agricultural chemicals
|