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Base de datos CISDOC

ID (ISN) del documento51404
Número CIS 89-576
ISSN - Título de la serie 0016-9900 - Gigiena i sanitarija
Año 1987
Número de serie
Autor(es) Moraru L.E., Girenko D.B., Klisenko M.A.
Título Chromatographic methods of determination of nitrogen and phosphorus-containing pesticides in air
Título original Hromatografičeskie metody opredelenija azot-fosforsoderžaščih pesticidov v vozduhe [en ruso]
Información bibliográfica Apr. 1987, No.4, p.53-54. Illus. 4 ref.
Resumen Conditions were determined for the collection, separation and quantitation of 4 organophosphorus pesticides that may be present in workplace air. 20L of air is drawn through a paper disc backed by polyurethane foam. The disc and foam are extracted with acetone and the extract is concentrated. A sample of the concentrate may be subjected to gas chromatography on a column of 5% Se-30 on Chromaton N-AW at 190 or 210°C (flame photometric or thermal ionisation detector), or to thin-layer chromatography on silica gel with hexane-acetone mixtures; after visualisation of spots with Dragendorff's reagent or silver nitrate, the diameters of the spots are measured. The limit detection in air of actellic, pirimiphos ethyl and pyridafenthion is 0.1mg/m3; for hostaquick, 0.2mg/m3. Error limits are 15.5-19.6%.
Descriptores (primarios) hostaquick; pesticidas; toma de muestras y análisis; dosificación en el aire; pirimifós etilo; cromatografía por gas líquido; cromatografía en capa delgada; pirimifós-metil; piridafentión
Descriptores (secundarios) valoración de la higiene del trabajo; valoración del método
Tipo de documento D - Artículos periódicos
Tema(s) Agricultura, pesca, cría de ganado
Broad subject area(s) Riesgos químicos
Navegación por categoria(s) Esters and salts
Agricultural chemicals