Document ID (ISN) | 30452 |
CIS number |
78-1969 |
ISSN - Serial title |
0300-581X - Arbeitsmedizin - Sozialmedizin - Präventivmedizin |
Year |
1978 |
Convention or series no. |
|
Author(s) |
Mundt W., Angerer J., Maassen J. |
Title |
Determination of arsenic in urine by flameless atomic absorption spectrometry |
Original title |
Bestimmung von Arsen im Harn mit Hilfe der flammenlosen Atomabsorptionsspektrometrie [in German] |
Bibliographic information |
Mar. 1978, Vol.13, No.3, p.62-64. Illus. 25 ref. |
Abstract |
Description of a method of determination particularly well suited for early screening for arsenic poisoning. The method is based on the conversion of arsenic in urine into arsine by reduction, using sodium borohydride, and on the thermal decomposition of arsine into elemental arsenic, which appears in the atomic absorption spectrometer. Description of preparation of the sample, method of determination, set-up required, reagents and results of recovery tests. Reliability criteria of the method are shown in a table. The limit of detection is 14µgAs/l urine; the recovery percentage is 90-100%. |
Descriptors (primary) |
arsenic; determination in urine; atomic absorption spectrometry |
Descriptors (secondary) |
sample processing; description of technique; urine monitoring |
Document type |
- |
Subject(s) |
Toxic and dangerous substances
|
Broad subject area(s) |
|
Browse category(ies) |
Arsenic and compounds Inorganic substances
|