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CISDOC database

Document ID (ISN)30452
CIS number 78-1969
ISSN - Serial title 0300-581X - Arbeitsmedizin - Sozialmedizin - Präventivmedizin
Year 1978
Convention or series no.
Author(s) Mundt W., Angerer J., Maassen J.
Title Determination of arsenic in urine by flameless atomic absorption spectrometry
Original title Bestimmung von Arsen im Harn mit Hilfe der flammenlosen Atomabsorptionsspektrometrie [in German]
Bibliographic information Mar. 1978, Vol.13, No.3, p.62-64. Illus. 25 ref.
Abstract Description of a method of determination particularly well suited for early screening for arsenic poisoning. The method is based on the conversion of arsenic in urine into arsine by reduction, using sodium borohydride, and on the thermal decomposition of arsine into elemental arsenic, which appears in the atomic absorption spectrometer. Description of preparation of the sample, method of determination, set-up required, reagents and results of recovery tests. Reliability criteria of the method are shown in a table. The limit of detection is 14µgAs/l urine; the recovery percentage is 90-100%.
Descriptors (primary) arsenic; determination in urine; atomic absorption spectrometry
Descriptors (secondary) sample processing; description of technique; urine monitoring
Document type -
Subject(s) Toxic and dangerous substances
Broad subject area(s)
Browse category(ies) Arsenic and compounds
Inorganic substances